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By J. D. Smith (auth.), A. McKillop, J. D. Smith, I. J. Worrall (eds.)

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Et a/, J. Am. Chem. , 1969, 91, 2538. 240 Cyclic dimer. Dimer: [14740-50-2]. ltrimethylsi/anolato )dialuminum. 480 Colour1ess cryst. 5°. 5°, Bp1 35° sub I. Stable to 200°. , J. Organomet. 136 Dimeric. Dimer: [ 15282-26-5]. l- (P,P,Ptrimethylphosphineimi dato )dialuminu m. 510 CwH32AizN 2Si 2 Whitc solid. Mp 7X-9°. Schmidbaur, H. et al. Angew Chem, /111. f:'d. , 1962. I. , J. Chem. Soc, 1963. , Angew. , lnt. , Chem. , 1966,99. 21n (pmr. q·nth. pmr) Al-00131 Trimethyl[thiobis [methane ]]aluminum.

150°. 144 Dimeric. Dimer: [50677-84-4]. l-methanesulfinato-O:O')tetramethyldialuminum, 9Ct. M. et a/, Can. J. , 1970, 48, I 093. 035 Cryst. M p 200-5°. Forms liq. complex with EtzO. 046 Prepd. in situ. Reagent for the prepn. of methylselenol esters (useful as acy1-transfer reagents). Also acts as a 1-acylethenyl anion equiv. in conjugate additions with enones. 083 Colourless, air-sensitive cryst. (C 6 H 6 ). Mp 144-5°. K salt: [53108-65-9]. 192 Colourless, air-sensitive cryst. Mp 202-5°. P. et a/, J.

Et al, J. Am. Chem. , 1942. T. et al, J. Chem. , Angew. , lnt. Ed. T. et al, J. Am. Chem. R. et a/, J. Chem. 442 Mp 100-2°. 214 Monomeric. White solid. Sol. CS 2 , C 6H 6 . Mp 103-4°. OJ 40-5° subl. T. et al, J. Am. Chem. E. et al, J. Chem. 101 Associated in hydrocarbons and ethers. Catalyst for stereospecific polymerisation of propylene oxide. 252 Mp -16°. Dec. 912 (ion) Air- and moisture-sensitive. Li sa/t: [62166-60-3]. 853 Prepd. and characterised spectroscopically in soln. Ueyama, N. et al, Inorg.

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