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By Cotton F., Wilkinson G., Murillo C., Bochmann M.

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I Waste from Purex process I Precipilole "Zr. 0M No2C03. Extroction 01 TcO; with pyridine I Precipitole %, Ca, Bo carbonates to e used for seporoting "Sr Precipitotion of olkoline eorth metols with No2 LO3 L I Precipitate Fe(OHI3 + Ru t - Reduction of TcO; with N2H,. 99 % Fig. A Schcmt: of the extraction of""Tc from a Purcx process waste solution [18]. The waste solution (Fig. A) is evaporated and the cake containing ''%r and 'I5Nb is removed. To separate Ru. iron(II1) hydrated oxide is precipitated with ammonia.

And Y. Alhinsaon. Kadiochim. 321-327 (1092) (311 V. F. Pcretrukhin. T. V. Khizhnynk. N. S. yalikova. and K. E. German. M. Milton. K. J. Cornett [33] E. A . liondietti and C. W. 1 [34J K. E. Meycr, W. D. Arnold and A. Vezina, Radiochim. 79. 1337 1340 (1979) d G. D. O’Kelly, Radiochim. 55. 351 R. Allnrd. 11. K i p t s i . and U. Xmtenfclt. Radiochcm. Radioanal. 223-230 ( I 979) 1361 K. 1 I. Liescr and C. Bauschcr. Radiochim. W. Golchert and J. Sedlet, Anal. Chcm. 41,669-671 (1969) [38] M. 11ttrep.

D. Arnold and A. Vezina, Radiochim. 79. 1337 1340 (1979) d G. D. O’Kelly, Radiochim. 55. 351 R. Allnrd. 11. K i p t s i . and U. Xmtenfclt. Radiochcm. Radioanal. 223-230 ( I 979) 1361 K. 1 I. Liescr and C. Bauschcr. Radiochim. W. Golchert and J. Sedlet, Anal. Chcm. 41,669-671 (1969) [38] M. 11ttrep. A. Enochs. and L. 11. BroL. En\-iron. Sci. Technol. 5,344-345 (1971) [39] S. Foti. E. Delucchi. and V. Akainian, Anal. Chim Acta 6U. 261-268 (1972) 1401 S. Fotl, E. Iklucchi. and L’. Akamian, Anal. Chim Acta 60.

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