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Verghese, J. Indian Chem. , 1975, 52, 175. 243 F. Bohlmann, J. Jacob, and M. Grenz, Chem. , 1975, 108, 433. 244 F. Bohlmann, C. Zdero, and M. Grenz, Chem. , 1975, 108, 2822. 245 M. Shibasaki, S. Terashima, and S. Yarnada, Chem. and Pharm. Bull. (Japan), 1975, 23. 279. *4h R. S. Becker, S. Berger, D . K. Dalling, D. M . Grant, and R. J. Pugmire, J. Amer. Chem. ,1974,96, 7008. 247 L. E. Brady, D. H. Williams, S. C. Traynor, and K . J . Crowley. Org. Mass Spectrometry, 1975,10, 1 16. 24x W. Cocker, K.

Zabza, C. Wawrzenczyk, and H. Kuczynski, Bull. Acad. polon. , Sir. Sci. , 1974, 22, 855 (Chem. , 1975,82, 73 196 has formulae IV and VI incorrect); cf Vol. 4, pp. 37, 51, 66. I. Uzarewicz and A. , 1975,49, 1113. E. Segiet-Kujawa and A. , 1974, 48, 2303. V. P. Yur'ev, A. V. Kuchin, T. Yakovleva, and G. A. Tolstikov, Zhur. , 1974,44,2084 (Chem. , 1975,82, 16 936). 1. Uzarewicz and A. , 1975, 49, 409 (Chem. , 1975, 83, 10 433 is incorrect). 44 Terpenoids and Steroids (225; R = 2-ketocyclopentyl), which is the sole product of oxidation using di-t-butyl Similarly di-t-butyl peroxide-catalysed free-radical addition of tetraas hydrothiophen to P-pinene yields (225; R = tetrahydr0thiophen-2-y1),~~~ expected from the previously reported diethyl phosphite addition (Vol.

Aso, Nippon Kagaku Kaishi, 1975, 866. G. Mehta and S. K. Kapoor, J. , 1974, 80, 213. g. (19 1)],298the synthesis of camphor-en01 trimethylsilyl ether,299and the stereochemistry of 2chloro-2-nitrosobicyclo[2,2, l l h e p t a n e ~Two . ~ ~ further ~ papers on the condensation of phenols with ~ a m p h e n e ~and ~ ~with . ~ ~fenchene301 ' as a function of acidic catalysis have appeared (cf. Vol. 2, p. 47; Vol. 4, p. 44; Vol. 5 , p. 36). r. chemical shifts in bicyclo[3,1, llheptanes support other known conformational evidence and confirm that cis-pinane and cis-myrtanol(209; X = OH) have a bridged-boat conformation, that trans-myrtanol has a bridged-chair conformation, and that trans-2-pinanol and myrtenol (210; X = OH) have Y-shaped conformations; verbenone (21 l ; R',R2 = 0),and trans-verbenol(21 l ;R' = H, R2= OH) give anomalous results which may be due to a conjugation effect; the bridged-chair conformation of nopinone (cf.

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